中国激光, 2010, 37 (8): 2149, 网络出版: 2010-08-13
激光微熔覆制备SnO2气敏膜及其性能研究
Experimental Study of SnO2 Gas-Sensing Film Fabricated by Laser Micro-Cladding and Its Corresponding Characteristics
摘要
以纳米氧化锡(SnO2)粉末为原料,有机溶剂为载体,配置了SnO2浆料,通过激光微熔覆技术在氧化铝基板上制备了SnO2气敏膜。采用X射线衍射(XRD)和场发射扫描式电子显微镜(FE-SEM)分析研究了激光功率对SnO2气敏膜微观结构和气敏特性的影响规律。实验表明,随着激光功率的升高,纳米SnO2的晶粒逐渐长大,气敏膜对乙醇气体的灵敏度逐渐降低;激光微熔覆制备的气敏膜对体积分数为2×10-3乙醇气体的灵敏度最高达到8.6,与传统丝网印刷工艺制备的气敏膜性能相当。
Abstract
SnO2 gas-sensing film is prepared on alumina substrate by laser micro-cladding SnO2 paste,which is obtained by mixing SnO2 nanoparticles with organic solvent. The effect of laser power on microstructure and gas-sensing properties of gas-sensing film are researched by X-ray diffraction (XRD) and field scanning electron microscope (FE-SEM). The results show that the grain sizes of SnO2 film gradually increase with raising laser power,while gas sensitivity to ethanol vapor decreases steadily. The gas sensitivity to 2×10-3 ethanol vapor of gas-sensing film fabricated by laser micro-cladding reaches a maximum value of 8.6,whose performance is equivalent to traditional screen-printed gas-sensing film.
蔡志祥, 曾晓雁. 激光微熔覆制备SnO2气敏膜及其性能研究[J]. 中国激光, 2010, 37(8): 2149. Cai Zhixiang, Zeng Xiaoyan. Experimental Study of SnO2 Gas-Sensing Film Fabricated by Laser Micro-Cladding and Its Corresponding Characteristics[J]. Chinese Journal of Lasers, 2010, 37(8): 2149.