光散射学报, 2009, 21 (4): 322, 网络出版: 2014-01-21
R-(+)-α-苯乙胺基草酰肼的拉曼光谱研究
Study of RS of R-(+)-α-Phenylethylamine Oxalylhydrazide
摘要
酰肼类的衍生物是制备光学纯螺二酮的一种重要手性拆分剂, 因此, 对酰肼类衍生物结构研究就显得尤为重要。在本文中我们对手性拆分剂R-(+)-α-苯乙胺基草酰肼进行了拉曼光谱测试分析, 并对主要的谱峰进行了归属, 进一步证实了它的结构。
Abstract
Hydrazide derivatives is a kind of chiral separation reagent which is important in preparing optically pure spiro-dione, so it is very significant to the research of the structure of hydrazide derivatives. Chiral separation reagent R-(+)-α-phenylethylamine oxalylhydrazide was studied by Raman spectroscopy in this paper, and its vibration wavenumbers were assigned to further confirmed its structure.
李为娇, 刘丽琴, 余洁, 赵玥萍, 刘自纯, 李文嘉, 沈爱国, 叶勇. R-(+)-α-苯乙胺基草酰肼的拉曼光谱研究[J]. 光散射学报, 2009, 21(4): 322. LI Wei-jiao, LIU Li-qing, YU Jie, LIU Zi-chun, LI Wen-jia, ZHAO Yue-ping, SHEN Ai-guo, YE Yong. Study of RS of R-(+)-α-Phenylethylamine Oxalylhydrazide[J]. The Journal of Light Scattering, 2009, 21(4): 322.