半导体光电, 2015, 36 (5): 760, 网络出版: 2015-11-30
非水溶胶凝胶法制备纳米二氧化钛及其抑菌性能研究
Preparation and Its Antibacterial Performance of Titania Nanoparticles by Nonaqueous SolGel Method
TiO2纳米颗粒 非水溶胶凝胶法 制备 表征 抑菌性能 TiO2 nanoparticles nonaqueous solgel preparation characterization antibacterial performance
摘要
以四氯化钛为钛源,叔丁醇为溶剂,采用非水溶胶-凝胶法制备了TiO2纳米颗粒,利用红外光谱(FTIR)、X射线衍射(XRD)、扫描电镜(SEM)和透射电镜(TEM)等技术手段对其进行了结构表征。基于定量菌落计数法考查了TiO2纳米颗粒对大肠杆菌和枯草杆菌的抑菌特性。结果表明,通过该方法合成的TiO2纳米颗粒粒径小,对这两种细菌的抑菌率都在93%以上,具有良好的抑菌效果。同时,简要分析了纳米TiO2抑菌机理,并对TiO2光催化材料的未来发展趋势进行了展望。
Abstract
TiO2 nanoparticles were prepared with titanium tetrachloride as the titanium source and tertbutanol as the solvent via a nonaqueous solgel method. The material was characterized by Xray diffraction (XRD),fourier transform infrared spectroscopy (FTIR),scanning electron microscopy (SEM),transmission electron microscopy (TEM) and high resolution transmission electron microscopy (HRTEM),respectively. Its antibacterial activity against escherichia coli and bacillus subtilis was investigated by the qualitative colony counting method. The results suggest that the TiO2 nanoparticles have the advantages of small particle size and an excellent antibacterial performance,the antibacterial rate to escherichia coli and bacillus subtilis is over 93%. Meanwhile,the antibacterial mechanism of TiO2 nanoparticles was investigated and the development in the future of titania photocatalytic materials was prospected.
杨志广, 赵朗, 李晓东, 王晓璐, 景志红. 非水溶胶凝胶法制备纳米二氧化钛及其抑菌性能研究[J]. 半导体光电, 2015, 36(5): 760. YANG Zhiguang, ZAHO Lang, LI Xiaodong, WANG Xiaolu, JING Zhihong. Preparation and Its Antibacterial Performance of Titania Nanoparticles by Nonaqueous SolGel Method[J]. Semiconductor Optoelectronics, 2015, 36(5): 760.