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强激光辐照前后钕玻璃中铂金颗粒夹杂物的电子探针显微分析

Electron Probe Micro-Analysis for Platinum Particle Inclusions in Nd∶Glass Before and After Intense Laser Irradiation

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摘要

采用电子探针显微分析(EPMA)技术分析和研究了强激光辐照前后连续熔炼钕玻璃中铂金颗粒的各种形态。强激光辐照后的铂金颗粒夹杂物呈现出3种典型的EPMA形貌, 这是铂金颗粒吸收激光能量引起的热应力和蒸气压共同作用的结果, 钕玻璃的热力学性质对其形态也有一定影响。对比锆和锡夹杂物的EPMA分布特性可以发现铂、锆、锡被共同包裹的现象。

Abstract

The electron probe micro-analyzer (EPMA) technology is used to analyze and study various forms of platinum (Pt) particle inclusions in continuous-smelted Nd∶glass before and after intense laser irradiation. After intense laser irradiation, platinum particle inclusions exhibit three typical EPMA morphology. Their forms come from the joint result of the thermal stress and vapor pressure caused by platinum particles absorbing laser energy. The thermodynamic properties of Nd∶glass also have an effect on the morphology. The phenomenon of Pt-Zr-Sn being co-wrapped is found by comparing the EPMA distribution characteristics of zirconium and stannum impurity inclusions.

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中图分类号:TQ171

DOI:10.3788/cjl201946.0303001

所属栏目:材料与薄膜

基金项目:国家重点专项钕玻璃基金

收稿日期:2018-11-15

修改稿日期:2018-12-13

网络出版日期:2018-12-21

作者单位    点击查看

程继萌:中国科学院上海光学精密机械研究所高功率激光单元技术研发中心, 上海 201800中国科学院大学材料与光电研究中心, 北京100049
温磊:中国科学院上海光学精密机械研究所高功率激光单元技术研发中心, 上海 201800
周秦岭:中国科学院上海光学精密机械研究所高功率激光单元技术研发中心, 上海 201800
倪加川:中国科学院上海光学精密机械研究所高功率激光单元技术研发中心, 上海 201800
陈伟:中国科学院上海光学精密机械研究所高功率激光单元技术研发中心, 上海 201800
胡丽丽:中国科学院上海光学精密机械研究所高功率激光单元技术研发中心, 上海 201800

联系人作者:陈伟(weichen@siom.ac.cn)

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引用该论文

Cheng Jimeng,Wen Lei,Zhou Qinling,Ni Jiachuan,Chen Wei,Hu Lili. Electron Probe Micro-Analysis for Platinum Particle Inclusions in Nd∶Glass Before and After Intense Laser Irradiation[J]. Chinese Journal of Lasers, 2019, 46(3): 0303001

程继萌,温磊,周秦岭,倪加川,陈伟,胡丽丽. 强激光辐照前后钕玻璃中铂金颗粒夹杂物的电子探针显微分析[J]. 中国激光, 2019, 46(3): 0303001

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