激光技术, 2023, 47 (2): 286, 网络出版: 2023-04-12  

基于3维荧光光谱测定白酒年份酒的年份

Determination of the age of aged Baijiu based on 3-D fluorescence spectroscopy
作者单位
1 江南大学 理学院, 无锡 214122
2 江苏省轻工光电工程技术研究中心, 无锡 214122
摘要
为了能够快速准确地检测白酒年份酒的年份, 采用了平行因子算法和光谱相似度算法对白酒年份酒与基酒的3维荧光光谱进行分析, 分别建立了高年份基酒体积分数的测定函数和年份酒年份测定函数。结果表明, 高年份基酒体积分数测定误差不超过0.02, 平均加标回收率为100.28%, 年份测定误差小于1年; 基于3维荧光光谱快速测定白酒年份酒年份的方法, 解决了由于3种基酒配制年份酒的3维荧光光谱复杂性而导致的年份酒年份鉴别困难问题。该研究为多种基酒配制年份酒的年份检测问题和其中基酒体积分数的确定提供了参考。
Abstract
In order to detect the age of aged Baijiu quickly and accurately, 3-D fluorescence spectra of aged Baijiu and base wine were analyzed by parallel factor algorithm and spectral similarity algorithm. The determination functions of volume fraction of high age base wine and age determination functions of aged Baijiu were established respectively. The results show that the determination error of volume fraction of high age base wine did not exceed 0.02, the average spiked recovery was 100.28%, and the error of age determination was less than 1 year; the method based on 3-D fluorescence spectra for rapid determination of age of aged Baijiu solved the difficulty of age identification due to the complexity of 3-D fluorescence spectra of 3 base wine formulations of aged Baijiu. This study provides a reference for the problem of age detection of aged Baijiu formulated with multiple base wines and the determination of the volume fraction of base wine among aged Baijiu.
参考文献

[1] LIU H L, SUN B G. Effect of fermentation processing on the flavor of Baijiu[J]. Journal of Agricultural and Food Chemistry, 2018, 66(22): 5425-5432.

[2] HONG J X, TIAN W J, ZHAO D R. Research progress of trace components in sesame-aroma type of Baijiu[J]. Food Research International, 2020, 137:109695.

[3] ZHENG X W, HAN B Z. Baijiu, Chinese liquor: History, classification and manufacture[J]. Journal of Ethnic Foods, 2016, 3(1):19-25.

[4] WANG X X, FAN W L, XU Y. Comparison on aroma compounds in Chinese soy sauce and strong aroma type liquors by gas chromatography-olfactometry, chemical quantitative and odor activity values analysis[J]. European Food Research and Technology, 2014, 239(5):813-825.

[5] SONG X B, ZHU L, JING S, et al. Insight into the role of 2-methyl-3-furanthiol and 2-furfurylthiol as markers for the differentiation of Chinese light, strong and soy sauce aroma types Baijiu[J]. Journal of Agricultural and Food Chemistry, 2020, 68(30): 7946-7954.

[6] DENG Y H, XIONG A Y, ZHAO K, et al. Mechanisms of the regulation of ester balance between oxidation and esterification in aged Baijiu[J]. Scientific Reports, 2020, 10(1):17169.

[7] ZHU L, WANG X L, SONG X B, et al. Evolution of the key odo-rants and aroma profiles in traditional laowuzeng Baijiu during its one-year ageing[J]. Food Chemistry, 2020, 310:125898.

[8] DONG W, GUO R N, SUN X T, et al. Assessment of phthalate ester residues and distribution patterns in Baijiu raw materials and Baijiu[J]. Food Chemistry, 2019, 283:508-516.

[9] CHINA ALCOHOLIC DRINKS ASSOCIATION. Group standards for aged Baijiu[EB/OL]. (2019-06-18)[2022-04-17]. https://www.cada.cc/Item/361.aspx(in Chinese).

[10] ZHANG Y, GU J, MA C Q, et al. Flavor classification and year prediction of Chinese Baijiu by time-resolved fluorescence[J]. A-pplied Optics, 2021, 60(19):5480-5487.

[11] WANG G X, WANG H Y, WANG H, et al. Study on the recognition of liquor age of gujing based on Raman spectra and support vector regression[J]. Spectroscopy and Spectral Analysis, 2016, 36(3):729-735(in Chinese).

[12] ZHANG M M, LU Y X, ZHAO Zh G, et al.Rapid discrimination of diffe-rent years of brewing liquor by gas chromatography-ion mobility spectroscopy combined with chemometrics method[J]. Science and Technology of Food Industry, 2021, 42(14):226-232(in Ch-inese).

[13] DAI H P, JIA J J, FAN Y, et al. Four-channel fluorescent sensor array based on various functionalized CdTe quantum dots for the discrimination of Chinese Baijiu[J]. Spectrochimica Acta , 2021, 252:119513.

[14] SONG X Sh, CHEN G Q, ZHU Zh W, et al. Determination of vo-lume fraction of acetic acid in Chinese aged liquor by 3-D fluore-scence spectrometry[J]. Laser Technology, 2018, 42(4):531-535(in Chinese).

[15] LIU M H, CHEN G Q, XIAO R J, et al. Classification of milk be-verages based on 3-D fluorescence spectroscopy[J]. Laser Technology, 2021, 45(3):303-306(in Chinese).

[16] GU J, CHEN G Q, ZHANG X H, et al. Classification and year prediction of Chinese liquors based on wavelet decomposition and factor analysis[J]. Spectroscopy and Spectral Analysis, 2018, 38(8):2511-2515(in Chinese).

[17] ZHU W H, CHEN G Q, ZHU Zh W, et al. Year prediction of a mild aroma Chinese liquors based on fluorescence spectra and quantum genetic algorithm[J]. Spectroscopy and Spectral Analysis, 2017, 37(5):1431-1436(in Chinese).

[18] LI R, CHEN G Q, ZHU Ch, et al. Quantitative analysis of two food colors using excitation-emission matrix spectra coupled with parallel factor algorithm[J]. Spectroscopy and Spectral Analysis, 2014, 34(1):111-115(in Chinese).

[19] WANG Sh T, LI M Sh, WANG Y T, et al. Qualitative and quantitative analysis of PAHs based on three-dimensional fluorescence spectroscopy and PARAFAC[J]. Spectroscopy and Spectral Analysis, 2020, 40(2):494-500(in Chinese).

[20] CHEN X Y, ZHANG K, KONG D M. Three-dimensional fluore-scence partial derivative spectroscopy combined with parallel factor algorithm for detection of mixed oil[J]. Spectroscopy and Spectral Analysis, 2021, 41(11):3506-3511(in Chinese).

[21] ZHANG Y, CHEN G Q, GU J, et al. A theoretical study on dime-rization and dissociation of acetic acid in ethanol solvent[J]. Computational & Theoretical Chemistry, 2020, 1191(25):113029.

[22] BURNEAU A, GNIN F, QUILS F. Ab initio study of the vibrational properties of acetic acid monomers and dimers[J]. Physical Chemistry Chemical Physics, 2000, 2(22):5020-5029.

王国宇, 陈国庆, 郭森琪, 韦一韬, 王子睿, 李晓琳. 基于3维荧光光谱测定白酒年份酒的年份[J]. 激光技术, 2023, 47(2): 286. WANG Guoyu, CHEN Guoqing, GUO Senqi, WEI Yitao, WANG Zirui, LI Xiaolin. Determination of the age of aged Baijiu based on 3-D fluorescence spectroscopy[J]. Laser Technology, 2023, 47(2): 286.

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