激光选区熔化成形TC4钛合金热处理后微观组织和力学性能 下载: 1609次
Microstructure and Mechanical Properties of TC4 Titanium Alloy Formed by Selective Laser Melting After Heat Treatment
1 南京理工大学机械工程学院, 江苏 南京 210094
2 南京理工大学数控成形技术与装备国家地方联合实验室, 江苏 南京 210094
图 & 表
图 1. SLM成形TC4钛合金圆柱状拉伸件
Fig. 1. Cylindrical drawing part of TC4 titanium alloy formed by SLM
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图 2. SLM成形TC4钛合金拉伸件实物图
Fig. 2. Physical picture of drawing part of TC4 titanium alloy formed by SLM
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图 3. 未热处理试样的微观组织。(a) OM照片(亮色部分为α'相,暗色部分为β相);(b) SEM照片
Fig. 3. Microstructure of untreated sample. (a) OM photo (light part is α' phase and dark part is β phase); (b) SEM photo
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图 4. 840 ℃/2 h/AC退火处理后TC4钛合金的显微组织。(a) OM照片(亮色部分为α相,暗色部分为β相);(b) SEM照片
Fig. 4. Microstructure of TC4 titanium alloy after 840 ℃/2 h/AC annealing treatment. (a) OM photo (light part is α phase and dark part is β phase); (b) SEM photo
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图 5. 940 ℃/1 h/WQ固溶处理后TC4钛合金的显微组织。(a) OM照片(亮色部分为α相,暗色部分为β相);(b) SEM照片
Fig. 5. Microstructure of TC4 titanium alloy after 940 ℃/1 h/WQ solution hardening. (a) OM photo(light part is α phase and dark part is β phase); (b) SEM photo
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图 6. 940 ℃/1 h/WQ+540 ℃/4 h/AC固溶时效处理后TC4钛合金的显微组织。 (a) OM照片(亮色部分为α相,暗色部分为β相);(b) SEM照片
Fig. 6. Microstructure of TC4 titanium alloy after 940 ℃/1 h/WQ+540 ℃/4 h/AC solution and aging treatment. (a) OM photo (light part is α phase and dark part is β phase); (b) SEM photo
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图 7. 不同热处理工艺下SLM成形TC4钛合金试样XRD图谱
Fig. 7. XRD patterns of TC4 titanium alloy samples produced by SLM after different heat treatment processes
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图 8. 不同热处理工艺下试样的断口形貌。(a)未热处理;(b) 840 ℃/2 h/AC; (c) 940 ℃/1 h/WQ;(d) 940 ℃/1 h/WQ+540 ℃/4 h/AC
Fig. 8. Fracture morphologies of samples after different heat treatment processes. (a) Untreated; (b) 840 ℃/2 h/AC; (c) 940 ℃/1 h/WQ; (d) 940 ℃/1 h/WQ+540 ℃/4 h/AC
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图 9. TC4钛合金试样残余应力测量点示意图
Fig. 9. Schematic of residual stress measurement points on TC4 titanium alloy sample
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图 10. 不同热处理工艺下TC4钛合金试样应力仿真。(a)未热处理;(b) 840 ℃/2 h/AC; (c) 940 ℃/1 h/WQ;(d) 940 ℃/1 h/WQ+540 ℃/4 h/AC
Fig. 10. Stress simulation of TC4 titanium alloy samples after different heat treatment processes. (a) Untreated; (b) 840 ℃/2 h/AC; (c) 940 ℃/1 h/WQ; (d) 940 ℃/1 h/WQ+540 ℃/4 h/AC
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表 1Ti6Al4V粉末的化学成分(质量分数,%)
Table1. Chemical compositions of Ti6Al4V power (mass fraction, %)
Element | Al | V | Fe | C | O | N | H | Mo | Mn | Cu | Sn | Y | Zr | Ti |
---|
Content | 5.500-6.750 | 3.500-4.500 | 0.140 | 0.007 | 0.130 | 0.007 | 0.002 | <0.050 | <0.050 | <0.050 | <0.050 | <0.050 | <0.050 | Bal. |
|
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表 2TC4钛合金SLM成形参数
Table2. Parameters of TC4 titanium alloy formed by SLM
Parameter | Laser power /W | Scanning speed /(mm·s
-1
) | Layer thickness /μm |
---|
Value | 180 | 1250 | 30 |
|
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表 3SLM成形TC4钛合金热处理条件
Table3. Heat treatment conditions for TC4 titanium alloy formed by SLM
Heat treatment mode | Heat treatment condition |
---|
Annealing | 840 ℃/2 h/AC | Solution hardening | 940 ℃/1 h/WQ | Solution and aging treatment | 940 ℃/1 h/WQ+540 ℃/4 h/AC |
|
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表 4不同热处理工艺下SLM成形TC4钛合金试样的力学性能
Table4. Mechanical properties of TC4 titanium alloy samples formed by SLM after different heat treatment processes
Heat treatment mode | Tensile strength /MPa | Yield strength /MPa | Elongation /% | Reduction of area /% |
---|
No heat treatment | 1130.55 | 1079.44 | 12.73 | 22.49 | 840 ℃/2 h/AC | 954.84 | 927.16 | 18.95 | 31.44 | 940 ℃/1 h/WQ | 880.67 | 841.37 | 15.95 | 15.36 | 940 ℃/1 h/WQ+540 ℃/4 h/AC | 901.93 | 890.31 | 15.35 | 10.89 |
|
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表 5不同热处理工艺下SLM成形TC4钛合金试样的残余应力实测及仿真值
Table5. Measured and simulated residual stresses of TC4 titanium alloy samples formed by SLM after different heat treatment processes
Heat treatment mode | Measured point | Residual stress /MPa |
---|
Measured | Simulated |
---|
| Point 1 | 175.5 | 183 | | Point 2 | 258.4 | 260 | Untreated | Point 3 | 113.3 | 127 | | Point 4 | 106.1 | 115 | | Point 1 | 58.6 | 59 | | Point 2 | 72.0 | 76 | 840 ℃/2 h/AC | Point 3 | 68.9 | 72 | | Point 4 | 59.3 | 55 | | Point 1 | 83.0 | 77 | | Point 2 | 94.3 | 95 | 940 ℃/1 h/WQ | Point 3 | 82.6 | 91 | | Point 4 | 73.1 | 71 | | Point 1 | 47.1 | 41 | | Point 2 | 59.9 | 55 | 940 ℃/1 h/WQ +540 ℃/4 h/AC | Point 3 | 49.5 | 51 | | Point 4 | 41.0 | 40 |
|
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肖振楠, 刘婷婷, 廖文和, 张长东, 杨涛. 激光选区熔化成形TC4钛合金热处理后微观组织和力学性能[J]. 中国激光, 2017, 44(9): 0902001. Xiao Zhennan, Liu Tingting, Liao Wenhe, Zhang Changdong, Yang Tao. Microstructure and Mechanical Properties of TC4 Titanium Alloy Formed by Selective Laser Melting After Heat Treatment[J]. Chinese Journal of Lasers, 2017, 44(9): 0902001.