人工晶体学报, 2020, 49 (4): 724, 网络出版: 2020-06-15  

反式二苯乙烯(TSB)晶体的溶液法生长研究进展

Research Progress on Crystal Growth of Trans-stilbene(TSB) Crystal by Solution Method
作者单位
1 北京工业大学材料科学与工程学院,北京 100124
2 北京工业大学固体微结构与性能研究所,北京 100124
3 北京玻璃研究院,北京 101111
摘要
反式二苯乙烯(TSB)晶体是一种可用于较强γ辐射下进行快中子检测的优良闪烁材料。由于溶液法得到的晶体在质量、性能等方面所表现的优越性,有必要对TSB晶体的溶液法生长技术进行系统研究。本文介绍了国内外关于TSB晶体的溶液降温法生长研究过程和取得的进展,对相应研究结果进行了分析,并提出了尚存在的问题。
Abstract
Trans-stilbene(TSB) crystal is an excellent scintillation material which can be used for fast neutron detection in strong γ ray environment. Because of the superiority of solution growth in crystal quality and performance, it is necessary to study the growth technique of TSB crystal in solution systematically. This paper has introduced the process and progress of TSB crystal growth by solution cooling method at home and abroad, analyzed the research results, and pointed out the problems that have yet to be solved in the growth process of TSB solution.
参考文献

[1] 杨 帆,任国浩.中子探测用闪烁体的研究进展[J].核电子学与探测技术,2009,29(4):895-901.

[2] 北京玻璃研究院.有机闪烁晶体的制备[J].原子能科学技术,1966(3):187-191.

[3] Hoekstra A, Meertens P, Vos A. Refinement of the crystal structure of trans-stilbene(Tsb) the molecular structure in the crystal line and gaseous phases[J].Acta Crystal lographica,1975, 31(12):2813-2817.

[4] 俞嗣皎,申敬廉,唐祖梅.有机闪烁体-芪晶体制备[J].核电子学与探测技术,1984,4(1):25-29.

[5] Arulchakkaravarthi A, Santhanaraghavan P, Ramasamy P. Crystal growth of trans-stilbene by vertical bridgman technique with modified growth vessels and its character isation[J].Journal of Crystal Growth,2001,224(1-2):89-94.

[6] Arulchakkaravarthi A, Santhanaraghavan P, Ramasamy P. Studies on microhardness and slip systems of bridgman grown trans-stilbene crystals[J].Materials Letters,2001,51(2):151-155.

[7] Carman L, Zaitseva N, Martinez H P, et al. The effect of material purity on the optical and scintillation properties of solution grown trans-stilbene crystals[J].Journal of Crystal Growth,2013,368:56-61.

[8] Zaitseva N, Glenn A, Carman L, et al. Scintillation properties of solution grown trans-stilbene single crystals[J].Nuclear Instruments and Methods in Physics Research,2015,789:8-15.

[9] Helmut Klapper, Natalia Zaitseva, Leslie Carman. X-ray to pographic study of growth defects of trans-stilbene crystals grown from golutions[J].Journal of Crystal Growth,2015,429:74-81.

[10] Carman M L, Glenn A M, Mabe A N. Solution growth of a ddeuterated trans-stilbene crystal for fast neutron detection[J].Journal of Crystal Growth,2018,498:51-55.

[11] Tony H Shin, PatrickL Feng, Joseph S, et al. Measured neutron light-output response for trans-stilbene and small molecule organic glass scintillators[J].Nuclear Instruments and Methods in Physics Research,2019,939:36-45.

[12] Sosa C S, Thompson S J, Chichester D L. Improved neutron gamma discrimination at low-light output events using conical trans-stilbene[J].Nuclear Instruments and Methods in Physics Research,2019,916:42-46.

[13] 任继齐,常新安,陈学安,等.反式二苯乙烯(TSB)的溶液法晶体生长[J].人工晶体学报,2017,46(3):404-409.

[14] 王淑君,常新安,陈学安,等.不同溶剂中TSB晶体的生长与形貌分析[J].硅酸盐学报,2018,46(7):957-963.

[15] 汤舟娅,常新安,陈学安,等.TSB溶液的回流热处理与晶体生长[J].硅酸盐学报,2019,49(10):1-6.

[16] 张克从,张乐潓.晶体生长科学与技术(上册)[M].北京:科学出版社,1997.

张开富, 常新安, 陈学安, 肖卫强, 张明荣. 反式二苯乙烯(TSB)晶体的溶液法生长研究进展[J]. 人工晶体学报, 2020, 49(4): 724. ZHANG Kaifu, CHANG Xinan, CHEN Xuean, XIAO Weiqiang, ZHANG Mingrong. Research Progress on Crystal Growth of Trans-stilbene(TSB) Crystal by Solution Method[J]. Journal of Synthetic Crystals, 2020, 49(4): 724.

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