掺镱大模场光子晶体光纤的研究进展 下载: 2182次特邀综述
Research Progress on Ytterbium-Doped Large Mode Area Photonic Crystal Fibers
1 中国科学院上海光学精密机械研究所强激光材料重点实验室, 上海 201800
2 中国科学院大学, 北京 100049
图 & 表
图 1. 高亮度掺镱LMA-PCF对芯棒的要求
Fig. 1. Requirements for mandrels in high brightness Yb-doped LMA-PCF
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图 2. MCVD工艺流程图[26]
Fig. 2. MCVD process flowchart[26]
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图 3. 纳米颗粒直接沉积制备芯棒工艺[35]
Fig. 3. Preparation of preform by DND process[35]
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图 4. 粉末烧结工艺图[37]
Fig. 4. Powder sintering process[37]
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图 5. 分相制备多孔工艺流程[43]
Fig. 5. Process of phase separation to prepare porous[43]
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图 6. 分相法制备稀土掺杂光纤工艺[45]
Fig. 6. Fabrication of rare earth doped optical fibers by phase separation method[45]
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图 7. 溶胶-凝胶工艺制备大模场掺镱光纤流程
Fig. 7. Fabrication of large mode ytterbium doped fiber process by sol-gel process
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图 8. (a) Yb/Al/P掺杂石英玻璃形成区;(b)玻璃形成区高硅区域局部放大图[24]
Fig. 8. (a) Glass forming region of Yb/Al/P doped silica glass; (b) magnified view of glass forming region in area with high content of SiO224
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图 9. Yb3+在YAP系列样品中的性能[29]。(a)吸收谱;(b)发射谱
Fig. 9. Performances of Yb3+ in YAP series samples[29]. (a) Absorption spectrum; (b) emission spectrum
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图 10. Yb3+/Al3+/P5+掺杂石英玻璃的Raman光谱[26]
Fig. 10. Raman spectra of Yb3+/Al3+/P5+ doped silica glass[26]
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图 11. Yb3+/Al3+/P5+共掺石英玻璃结构[26]
Fig. 11. Structure of Yb3+/Al3+/P5+ co-doped quartz glass[26]
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图 12. Yb2O3、Al2O3、P/Al的物质的量之比及AlPO4对石英玻璃折射率的影响[26,29,31]
Fig. 12. Effects of Yb2O3, Al2O3, P/Al ratio, and AlPO4 on refractive index of silica glass[26,29,31]
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图 13. 掺镱石英玻璃芯棒照片
Fig. 13. Photographs of Yb-doped quartz glass mandrels
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图 14. 光子晶体光纤的端面及纤芯成分分布。(a) PCF截面照片;(b)纤芯中Yb、Al、P、F元素EPMA线扫描图
Fig. 14. Photographs of photonic crystal fibers and composition distribution of fiber cores. (a) PCF cross-sectional photographs; (b) EPMA line scan maps of Yb, Al, P, and F elements in fiber core
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图 15. 激光放大系统及输出激光特性。 (a)主振荡功率放大系统;(b)脉冲放大平均功率随抽运光功率变化,插图分别为120 W和272 W时的光束质量
Fig. 15. Laser amplification system and output laser characteristics. (a) Main oscillator power amplifier system; (b) average pulse amplification power versus pump power. Insets are beam qualities at 120 W and 272 W, respectively
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图 16. 光子晶体光纤端面照片及激光放大性能。(a) 75 μm芯径的LMA-PCF端面SEM照片;(b)脉冲放大平均功率随抽运光功率变化
Fig. 16. Photo of photonic crystal fiber end face and laser amplification performance. (a) SEM photograph of large mode area PCF with 75 μm core diameter; (b) average pulse amplification power versus pump power
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图 17. 溶胶-凝胶法制备LMA-PCF的研究进展
Fig. 17. Development of LMA-PCF fabricated by sol-gel method
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表 1基于溶胶-凝胶法制备掺镱石英光纤的研究进展
Table1. Development of ytterbium doped silica fibers using sol-gel method
Time | Composition | Mole fractionof Yb2O3 /% | Fibertype | Corediameter /μm | Lasersystem | Averagepower /W | Peakpower /MW | M2 | Reference |
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2013 | Yb/Al | 0.3 | PCF | 30 | CW | 6.8 | - | - | [22] | 2013 | Yb/Al | 0.1 | PCF | 90 | CW | 81 | - | - | [23] | 2013 | Yb/Al/P | 0.05 | PCF | 35 | CW | 35 | - | - | [53] | 2015 | Yb/Al/P | 0.035 | DCFPCF | 3550 | CW | 3.246 | -- | 1.3- | [57] | 2016 | Yb/Al | 0.1 | PCF | 105 | MOPA | 255 | 1.2 | >10 | [54] | 2016 | Yb/Al/F | 0.05 | DCF | 50 | CW | 8 | - | 1.1 | [20] | 2017 | Yb/Al | 0.1 | PCF | 100 | MOPA | 310 | 1.5 | 5 | [59] | 2017 | Yb/Al/P/F | 0.075 | PCF | 50 | MOPA | 97 | 0.093 | 1.4 | [55] | 2019 | Yb/Al/P/F | 0.09 | PCF | 50 | MOPA | 272 | 0.266 | 2.2 | [51] | 2019 | Yb/Al/P/F | 0.15 | PCF | 75 | MOPA | 102 | 1 | 2.1 | [60] |
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表 2不同组分的掺镱石英玻璃芯棒特点
Table2. Characteristics of Yb-doped silica glass rods with different compositions
Core glass | Glass forming ability | Homogeneity | Refractive difference | Spectra properties | Reference |
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Yb/Al | Easy | 1×10-4 | Far larger than pure silica glass | Good | [22,52] | Yb/Al/P | Easy (with largerAl content than P) | 2×10-4 | (3-6)×10-4 | Great changes (withmuch larger P than Al) | [28-29,31] | Yb/Al/F | Easy | 2×10-4 | Almost equal to pure silica glass | Good | [20,30] | Yb/Al/P/F | Possible phaseseparation | 1×10-4 | Almost equal to pure silica glass | Good (with less Pcontent than Al) | [51,55-56] |
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表 3本课题组制备掺镱石英玻璃芯棒与Heraeus公司产品性能对比
Table3. Performance comparison between Yb-doped quartz glass mandrel prepared by our research group and Heraeus products
Specification | SIOM | Heraeus |
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Powder sintering | Sol-gel | SiCl4+H2O | Active glass rod diameter | >5 mm | >5 mm | Homogeneity | About1×10-4 | <2×10-4 | Codoping F | Yes | No | Codoping P | Yes | No | Core glass attenuation | >50 dB/km@1200 nm | <50 dB/km@1200 nm | Main application | Low NA ultra large mode fieldphotonic crystal fibers forpulse amplification | Ultra large core diameter claddingfiber for high average powerCW/pulsed fiber laser amplifier |
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于春雷, 王孟, 冯素雅, 王世凯, 王璠, 楼风光, 张磊, 陈丹平, 胡丽丽. 掺镱大模场光子晶体光纤的研究进展[J]. 激光与光电子学进展, 2019, 56(17): 170602. Chunlei Yu, Meng Wang, Suya Feng, Shikai Wang, Fan Wang, Fengguang Lou, Lei Zhang, Danping Chen, Lili Hu. Research Progress on Ytterbium-Doped Large Mode Area Photonic Crystal Fibers[J]. Laser & Optoelectronics Progress, 2019, 56(17): 170602.