In this work, a heavily Er-doped fiber with an 8 µm core diameter and a numerical aperture of 0.13 was prepared by the modified chemical vapor deposition (MCVD) technique combined with the sol-gel method. The background loss and absorption coefficient at 1530 nm were measured to be 20 dB/km and 128 dB/m, respectively. Thanks to the sol-gel method, the fiber showed a good doping homogeneity, which was confirmed through unsaturable absorption measurement. The net gains of three 25, 45, and 75-cm-long fibers were measured in the range of 1520 to 1600 nm, and the highest gain reached above 23 dB at both 1530 and 1560 nm in 25 and 75-cm-long fibers, respectively. The short-cavity laser performance was measured using centimeter-scale fibers. The maximum output power of 12 mW was demonstrated in a 6.5-cm-long active fiber with a slope efficiency of 20.4%. Overall, the prepared heavily Er-doped silica fiber is a promising item to be applied in a high-repetition-rate or single-frequency fiber laser.

A large-mode-area (LMA) ytterbium-doped photonic crystal fiber (PCF) with core NA of 0.034 and core diameter of 50 μm was made by the stack-and-draw technique. The core is formed by Yb³⁺/Al³⁺/F /P⁵⁺ co-doped silica glass containing 0.09 mol% Yb₂O₃ with an absorption coefficient at 976 nm up to 3.2 dB/m. The core glass with homogeneous distribution of Yb³⁺ ions and refractive index difference of 4 × 10 ⁴ compared with pure silica was prepared by the sol-gel method and heat homogenization at 2000°C. Laser power amplification of this LMA PCF was studied using a seed source of 21 ps pulse duration and 48.7 MHz repetition rate at 1030 nm wavelength. With pump power of 520 W, a maximum 272 W (266 kW peak power) quasi-single-mode laser output with M² of 2.2 was achieved in a 4.7 m fiber length bent at a diameter of 47 cm with slope efficiency of 52%, and no obvious mode instability, stimulated Raman scattering, or thermal damage on the end facet of the fiber were observed.

Induced loss at 633 nm is tested in Yb3+/Al3+ co-doped silica fiber by a core pumped with a 974 nm laser and probed with a 633 nm laser. The fiber is prepared by the modified chemical vapor deposition method combined with solution doping. Different power scales of pump light and probe light are used in the tests. It is found that there is a dynamic equilibrium between photobleaching induced by 633 nm probe light and photodarkening (PD) induced by 974 nm pump light. For the first time to our knowledge, the effect of 633 nm probe laser power on an induced loss test of Yb3+/Al3+ co-doped silica fiber is studied quantitatively. It suggests that as long as the 633 nm probe light power is less than 0.2 mW, the induced loss is mainly contributed by the PD effect of pumping light, and the deviation of induced loss is less than 5%.