Photonics Research, 2019, 7 (11): 11000B73, Published Online: Oct. 28, 2019  

Scanning electron microscopy as a flexible technique for investigating the properties of UV-emitting nitride semiconductor thin films Download: 807次

Author Affiliations
1 Department of Physics, SUPA, University of Strathclyde, Glasgow G4 0NG, UK
2 Tyndall National Institute, University College Cork, Cork T12 R5CP, Ireland
3 Institute of Solid State Physics, Technische Universität Berlin, 10623 Berlin, Germany
4 Ferdinand-Braun-Institut, Leibniz-Institut für Höchstfrequenztechnik, 12489 Berlin, Germany
5 Department of Electronic and Electrical Engineering, Centre of Nanoscience & Nanotechnology, University of Bath, Bath BA2 7AY, UK
6 Department of Electronic and Electrical Engineering, University of Sheffield, Sheffield S1 3JD, UK
7 Laser Components Department, Laser Zentrum Hannover e.V., 30419 Hannover, Germany
Figures & Tables

Fig. 1. ECCI micrograph from AlGaN thin film.

下载图片 查看原文

Fig. 2. (a) SE image of nPSS, (b) schematic of overgrowth of AlN on nPSS, and (c) ECCI micrograph from an AlN thin film. Inset is on the same scale but with higher resolution.

下载图片 查看原文

Fig. 3. EBSD maps from the AlN/nPSS thin film: (a) grain reference orientation deviation (GROD) map and (b) GROD axis map relative to the sample normal (c-axis, [0001] direction]) where the colors denote direction of in-plane rotation (i.e., around the c-axis). The red regions are rotated in the opposite direction to the blue regions as indicated.

下载图片 查看原文

Fig. 4. (a) Schematic of semi-polar GaN microrod template and overgrowth, indicating the distribution of stacking faults on the surface of the sample and the crystallographic directions. (b) ECCI micrograph revealing stacking faults. (c) Example CL spectra from a dark stripe and a bright stripe, respectively. The boxes on (d) indicate where the spectra were extracted from the CL dataset. (d) Integrated CL intensity image of the GaN near band edge (NBE) emission (3.15–3.50 eV) on the same scale as (e) but not from the same area. (e) Higher resolution ECCI micrograph revealing dislocations. (f) Integrated CL intensity image of the GaN near band edge (NBE) emission (3.15–3.50 eV) on the same scale as (e) but not from the same area.

下载图片 查看原文

Fig. 5. (a) Schematic of the sample structure. x=0.82 for the top 1.6 μm layer. (b) Atomic force microscopy image of the sample surface. (c) ECCI micrograph (the black brackets indicate “stripes” of higher dislocation density in the coalescence region). (d) Topographic image. (c) CL near band edge (NBE) peak intensity map. (d) NBE CL peak energy map. Images (c) to (f) were acquired from approximately the same region of the sample. The white arrows indicate the apexes of the hillocks. The CL peak intensity and peak energy were extracted from hyperspectral data.

下载图片 查看原文

Fig. 6. WDX maps of the intensities of (a) Ga Lα (left) and (c) Al Kα (right) X-rays, and (b) a backscattered electron image (center) of a micrometer-scale region of a c-plane AlGaN sample, with an average AlN content of 81%. The scale bar for X-ray intensities applies to both WDX maps, although with different absolute values.

下载图片 查看原文

Fig. 7. (a) Semi-log plot showing the measured Si content in the GaN layers, calibrated using the points where SIMS data is available (red data points). (b) Long qualitative scan for Si for the sample with lowest measured Si content 2.3×1017  cm3, using a TAP crystal showing the WDX Si peak.

下载图片 查看原文

C. Trager-Cowan, A. Alasmari, W. Avis, J. Bruckbauer, P. R. Edwards, B. Hourahine, S. Kraeusel, G. Kusch, R. Johnston, G. Naresh-Kumar, R. W. Martin, M. Nouf-Allehiani, E. Pascal, L. Spasevski, D. Thomson, S. Vespucci, P. J. Parbrook, M. D. Smith, J. Enslin, F. Mehnke, M. Kneissl, C. Kuhn, T. Wernicke, S. Hagedorn, A. Knauer, V. Kueller, S. Walde, M. Weyers, P.-M. Coulon, P. A. Shields, Y. Zhang, L. Jiu, Y. Gong, R. M. Smith, T. Wang, A. Winkelmann. Scanning electron microscopy as a flexible technique for investigating the properties of UV-emitting nitride semiconductor thin films[J]. Photonics Research, 2019, 7(11): 11000B73.

引用该论文: TXT   |   EndNote

相关论文

加载中...

关于本站 Cookie 的使用提示

中国光学期刊网使用基于 cookie 的技术来更好地为您提供各项服务,点击此处了解我们的隐私策略。 如您需继续使用本网站,请您授权我们使用本地 cookie 来保存部分信息。
全站搜索
您最值得信赖的光电行业旗舰网络服务平台!